Synthesis and Study of 7,12,17-Trioxa[11]helicene
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https://figshare.com/articles/dataset/Synthesis_and_Study_of_7_12_17_Trioxa_11_helicene/2103037
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Synthesis of the title compound 7,12,17-trioxa[11]helicene, a large oxygen-containing helicene, has been reported. The 11-membered heterohelicene was synthesized by a combination of two simple reactions involving oxidative coupling and dehydrative cyclization. The final helicene was characterized by single-crystal X-ray diffraction, fluorescence spectroscopy, and differential scanning calorimetric analysis.
创建时间:
2016-02-12



