Natrolite - Sample 2 NanED Round Robin, Data: ESR10

Natrolite

The following submission contains the data collection and processing of the dataset for the sample natrolite under the NanEd round-robin project. A single crystal was identified, and the rotation data acquisition technique was used to collect the dataset on the same crystal. The dataset was processed with XDS software. The table below summarizes the data collection parameters for the dataset. The following data is also in the data folder as a Word file.

Continuous Rotation:

General information:

Project

NanED (www.naned.eu)

ESR Project

ESR10 - Round Robin

Project Label

RR-2

Sample Label

RR-2_SU

Data set Label

RR-2

Instrumental:

Instrument

Transmission electron microscope JEOL 2100 LaB6

Radiation source

LaB6

Accelerating voltage

200 kV

Wavelength

0.0251 Å

Probe Type

Parallel beam

Beam Diameter

6 μm

Beam Convergence

Parallel beam, convergence <0.1mrad

Detector

Hybrid pixel detector ASI Timepix (bottom mounted)

Number of pixels in the image

512 x 512

Pixel size

55 µm x 55 µm

Effective camera length

250 mm

Calibration constant

0.004990 Å-1/pixel

Sample description:

Name

Natrolite

Chemical composition

Na2Si3Al2O10.(H2O)2

Sample source

Sample preparation

Powder crushed in an agate mortar and deposited on a Cu grid with lacey C film

Experimental:

Data Type

Electron diffraction data - 3D ED

Data collection method

Continuous Rotation

Temperature (K) used during data collection

293 K

Number of crystals contributing to the data set

1

Number of experimental frames

513

tilt range, tilt step, tilt per frame

 -48.35°-70.58°, 0.453°/s, 0.2318°/frame

Exposure time per frame

0.5

Software:

Software used for the data collection

Instamatic

Software used for processing

XDS

Authorship and bibliography

Author(s) of the data

Lei Wang (ESR 10)

Related data

Publication(s)

Files and data formats

Image folder

REDp: Folder containing images of the diffraction pattern from each frame

XDS: Folder containing images of the diffraction pattern from each frame

Image format

mrc and img

Additional folders/files

Crystal image : image of the crystal

cRED_log: log file of data collection

1.ed3d: input file for REDp

XDS.INP: input file for the program XDS

Notes:

*Project Label "RR-2" stands for Round Robin 2

*RR-2 contains 1 dataset.