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METHOD FOR PREPARING CELLULOSE NANOFIBRILS BY DEEP EUTECTIC SOLVENT PRETREATMENT

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国家林业和草原科学数据中心2023-02-12 更新2024-03-07 收录
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The disclosure provides a method for preparing cellulose nanofibrils by deep eutectic solvent pretreatment, characterized in that the method comprises: Si. Deep eutectic solvent pretreatment: a chemical pulp is added to the deep eutectic solvent to obtain a mixed solution; S2. Separation of the treated pulp fibers: water is added to the reaction system in step Sl to terminate the reaction, and then the pulp fibers are separated from the mixed solution; S3. High-pressure homogenization microfluidization: the pulp fibers separated in step S2 are formulated into a slurry having a particular slurry concentration, then subjected to high-pressure homogenization microfluidization, and then spray-dried to obtain a cellulose nanofibril product. In this disclosure, the preparation conditions are mild; the operation is simple; the cost is low; and the pollution is small; the used deep eutectic solvent can be recovered by methods such as rotary evaporation and the like and therefore can be reused; it is environmentally friendly, meets the standards of green chemical production, and has good practical application value.
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国家林业和草原科学数据中心
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2023-02-12
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