Publication raw data: Continuous-flow microreactor for Knoevenagel condensation of ethyl cyanoacetate with benzaldehyde. The effect of grafted amino groups on catalytic activity

Data for Publication: ChemPlusChemsample designation in the publication: M; M-N1; M-N2; M-N3; M-N4; M-N5File:ASAPFile format: *xlsx;*csvFigure 1, Table 1 in manuscriptData from nitrogen adsorption/desorption measurments.ASAP2020 Micromeritics; ASAP2020 softwereSamples degassed at 200 ◦C under vacuum for 24 h. Nitrogen adsorption at −196◦C. The specific surface area calculated using Braunauer, Emmet and Teller (BET) equation; micropore size using the Dubinin–Astakhov equation.File:FTIRFile format: *csvFigure 3 in manuscriptData from FTIR measurmentsNICOLET 6700 spectrometer; Thermo Fisher Scientific; OMNIC softwere; DRIFT (5% of sample in KBr); Spectra range 400–4000 cm−1; resolution 4 cm−1.File:TGFile format: *csvFigure 4, Table 2 in manuscriptData from thermogravimetric measurmentsStar 850, Mettler Toledo. Temperature range of 25-800 °C, heating ramp of 10 deg/min, air rate 60 ml/minFile:Catalytic ExperimentsFile format:*pdfFigure 5-10, Table 4 in manuscriptReports from GC chromatographyAgilent 7890A, flame ionization detector FID; capillary column HP5; Inlet temperature: 250◦C ; sample volume: 1um, split ratio: 5:1; oven temp: 40◦C-200o◦C He flow 6.5 ml/min; detector: temperature 300◦C; H2 flow:30 ml/min, Air flow:400ml/min