3D ED dataset of 1,3,5-triphenylbenzene

Continuous rotation 3D ED data collection of 1,3,5-triphenylbenzene (TPB). See the following table for additional details.

Project name
TPB_25032024

Instrumental

Instrument
ELDICO ED-1 electron diffractometer

Electron source

LaB6

Electron energy 
160 kV

Wavelength
0.02851 Å

Beam mode
pseudo-parallell

Beam diameter
750 nm

Detector
Dectris QUADRO

Detetor no. of pixels
512 x 512

Detetor pixel size
75 µm

Data collection mode
continuous rotation

Measurement temperature
298 K

Instrument control software
eldix, Version 4.3.1

Sample

Compound
1,3,5-triphenylbenzene

Chemical formula

C24H18

Sample source
commercial, 99+% purity

Grid
amorphous carbon on copper

Sample preparation
grinding of the sample between microscope slides and dry preparation on the grid

Files and data formats

Diffraction frame folders
03, 06, 07, 08

Diffraction frame format
.cbf

Additional files
subfolders with STEM images of the particles at different tilt angles

Comments
folder _full.zip contains the full measurement data, folder _recommended.zip already has frames removed which are affected by other crystals in the beam, shadowing by the grid bars, or beam damage