Natrolite - Sample 2 NanED Round Robin, Data: ESR10

Natrolite The following submission contains the data collection and processing of the dataset for the sample natrolite under the NanEd round-robin project. A single crystal was identified, and the rotation data acquisition technique was used to collect the dataset on the same crystal. The dataset was processed with XDS software. The table below summarizes the data collection parameters for the dataset. The following data is also in the data folder as a Word file. Continuous Rotation: General information: Project NanED (www.naned.eu) ESR Project ESR10 - Round Robin Project Label RR-2 Sample Label RR-2_SU Data set Label RR-2 Instrumental: Instrument Transmission electron microscope JEOL 2100 LaB6 Radiation source LaB6 Accelerating voltage 200 kV Wavelength 0.0251 Å Probe Type Parallel beam Beam Diameter 6 μm Beam Convergence Parallel beam, convergence <0.1mrad Detector Hybrid pixel detector ASI Timepix (bottom mounted) Number of pixels in the image 512 x 512 Pixel size 55 µm x 55 µm Effective camera length 250 mm Calibration constant 0.004990 Å-1/pixel Sample description: Name Natrolite Chemical composition Na2Si3Al2O10.(H2O)2 Sample source Sample preparation Powder crushed in an agate mortar and deposited on a Cu grid with lacey C film Experimental: Data Type Electron diffraction data - 3D ED Data collection method Continuous Rotation Temperature (K) used during data collection 293 K Number of crystals contributing to the data set 1 Number of experimental frames 513 tilt range, tilt step, tilt per frame -48.35°-70.58°, 0.453°/s, 0.2318°/frame Exposure time per frame 0.5 Software: Software used for the data collection Instamatic Software used for processing XDS Authorship and bibliography Author(s) of the data Lei Wang (ESR 10) Related data Publication(s) Files and data formats Image folder REDp: Folder containing images of the diffraction pattern from each frame XDS: Folder containing images of the diffraction pattern from each frame Image format mrc and img Additional folders/files Crystal image : image of the crystal cRED_log: log file of data collection 1.ed3d: input file for REDp XDS.INP: input file for the program XDS Notes: *Project Label "RR-2" stands for Round Robin 2 *RR-2 contains 1 dataset.