Epidote - Sample 1 NanED Round Robin, Data ESR3

General information: Project NanED (www.naned.eu) ESR Project ESR3 Instrumental: Instrument FEI TECNAI Radiation source FEG Accelerating voltage 200 kV Wavelength 0.0251 Å Acquisiton Method SAED Detector Eagle – CCD Camera Number of pixels in the image 2048 x 2048 Calibration constant (not corrected for Effective Camera length) 0.00182 Å-1/pixel Sample description: Name Epidote Chemical composition Ca2FexAl3-xSi3O13H Experimental: Data Type Electron diffraction data - 3D ED Data collection method Stepwise Temperature (K) used during data collection 293 K Number of crystals contributing to the data set 1 Number of experimental frames 351 tilt range, tilt step -35° to +35°, 0.2° Exposure time per frame 1s Software: Software used for the data collection TIA Software used for processing PETS2 Software used for Solution Jana Software used for refinement Olex2