3D ED dataset of 1,3,5-triphenylbenzene

Continuous rotation 3D ED data collection of 1,3,5-triphenylbenzene (TPB). See the following table for additional details. Project name TPB_25032024 Instrumental Instrument ELDICO ED-1 electron diffractometer Electron source LaB6 Electron energy 160 kV Wavelength 0.02851 Å Beam mode pseudo-parallell Beam diameter 750 nm Detector Dectris QUADRO Detetor no. of pixels 512 x 512 Detetor pixel size 75 µm Data collection mode continuous rotation Measurement temperature 298 K Instrument control software eldix, Version 4.3.1 Sample Compound 1,3,5-triphenylbenzene Chemical formula C24H18 Sample source commercial, 99+% purity Grid amorphous carbon on copper Sample preparation grinding of the sample between microscope slides and dry preparation on the grid Files and data formats Diffraction frame folders 03, 06, 07, 08 Diffraction frame format .cbf Additional files subfolders with STEM images of the particles at different tilt angles Comments folder _full.zip contains the full measurement data, folder _recommended.zip already has frames removed which are affected by other crystals in the beam, shadowing by the grid bars, or beam damage