Serum Lipids
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https://figshare.com/articles/Serum_Lipids/7579790/1
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Lipids were extracted from serum samples in methanol:dicholoromethane in the presence of internal standards by Metabolon, Inc. The extracts were concentrated under nitrogen and reconstituted in 0.25 mL of 10 mM ammonium acetate dichloromethane:methanol (50:50). The extracts were transferred to inserts and placed in vials for infusion-MS analysis, performed on a Shimazdu LC with nano PEEK tubing and the Sciex Selexlon-5500 QTRAP. Samples were analyzed via both positive and negative mode electrspray. The 5500 QTRAP scan was performed in MRM mode, with more than 1,100 MRMs.
提供机构:
figshare
创建时间:
2019-04-12



