Trapping a Discrete [R<sub>2</sub>Sn(μ-OH)SnR<sub>2</sub>] Motif. Synthesis and Structural Characterization of [{(Phen)(NO<sub>3</sub>)Me<sub>2</sub>Sn(μ-OH)SnMe<sub>2</sub>(NO<sub>3</sub>)(Phen)}{NO<sub>3</sub>}] (Phen = 1,10-Phenanthroline)
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The reaction of Me2SnCl2 with 2 equiv of silver nitrate in methanol followed by treatment with 2 equiv of water and 1 equiv of 4,4′-bipyridine in presence of 1,10-phenanthroline afforded the hydrolyzed product [(NO3)(Phen)Me2Sn(μ-OH)SnMe2(Phen)(NO3)]+[NO3]− (4), containing a [R2Sn(μ-OH)SnR2] unit where two diorganotin units are bridged by an unsupported hydroxide ligand.
创建时间：
2008-08-25
