Detangling Catalyst Modification Reactions from the Oxygen Evolution Reaction by Online Mass Spectrometry
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https://figshare.com/articles/dataset/Detangling_Catalyst_Modification_Reactions_from_the_Oxygen_Evolution_Reaction_by_Online_Mass_Spectrometry/4047786
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资源简介：
Here we showcase
the synthesis and catalytic response of the anionic
iridium(III) complex [IrCl3(pic)(MeOH)]− ([1]−, pic = picolinate) toward the
evolution of oxygen. Online electrochemical mass spectrometry experiments
illustrate that an initial burst of CO2 due to catalyst
degradation is expelled before the oxygen evolution reaction commences.
Electrochemical features and XPS analysis illustrate the presence
of iridium oxide, which is the true active species.
创建时间：
2016-10-31
