MicroED/3DED datasets of acetaminophen collected with a Ceta camera on Talos Arctica

Continuous rotation data sets were collected on a Talos Arctica (200 kev) equipped with a ceta camera. Each dataset was collected with an approximate flux of 0.17 e-/ Å2/s-1 which means a total exposure of 20.4 e-/Å2 for a 120-degree wedge of data. Delphi was used to rotate the crystal while TEM Imaging & Analysis (TIA) software was used to collect the data. Datasets were processed in DIALS directly without any conversion. The structure was solved to 0.84 Å with 99% of overall completeness by merging two datasets (attached). Experimental parameters are as follows: Accelerating voltage: 200 Kev Wavelength: 0.02508 Cameralength: 1012 mm Exposure time: 1 s Rotation speed: 1 degrees per second Rotation: 60 to -60 degrees Detector area: 4096 x 4096 (Bin 1) Pixel size: 14 µm Spot size: 8 C2 aperture: 50 µm SA aperture: 40 µm