An Efficient Synthesis Strategy to the Core Structure of 6–5–6–5–6-Membered Epipolythiodiketopiperazines

Figshare2016-02-17 更新2026-04-29 收录

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A concise route to the core structure 1 of 6–5–6–5–6-membered epipolythiodiketopiperazines is described. The strategy relies on construction of the pyrrolines by double nucleophilic opening of a bis(oxabicyclo[2.2.1]heptene) 2, obtained after bidirectional condensation of N,N′-diacetyldiketopiperazine (4) with aldehyde 3.

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2016-02-17

An Efficient Synthesis Strategy to the Core Structure of 6–5–6–5–6-Membered Epipoly­thiodiketo­pipera­zines

An Efficient Synthesis Strategy to the Core Structure of 6–5–6–5–6-Membered Epipolythiodiketopiperazines