Metal-Free sp3 C–H Bond Dual-(Het)arylation: I2-Promoted Domino Process to Construct 2,2-Bisindolyl-1-arylethanones
收藏Figshare2016-02-20 更新2026-04-29 收录
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https://figshare.com/articles/dataset/Metal_Free_sp_sup_3_sup_C_H_Bond_Dual_Het_arylation_I_sub_2_sub_Promoted_Domino_Process_to_Construct_2_2_Bisindolyl_1_arylethanones/2507470
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A molecular I2-promoted sp3 C–H bond dual-(het)arylation protocol was developed for the synthesis of 2,2-bisindolyl-1-arylethanones. Through a logical design, three mechanism-different reactions (iodination, Kornblum oxidation, and Friedel–Crafts reaction) were assembled in a single reactor. A variety of 2,2-bisindolyl-1-aryl ethanones were synthesized from simple and readily available aryl methyl ketones and indoles. In the reaction, metal, base, and ligand were all avoidable.
创建时间：
2016-02-20
