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HILIC Positive Mode Sample Raw Data

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DataCite Commons2025-05-01 更新2024-07-29 收录
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https://figshare.com/articles/dataset/HILIC_Positive_Mode_Sample_Raw_Data/19280114/1
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资源简介:
Samples (2-10 mg) were extracted with 2:5:2 CDCl3:CD3OD:H2O, ground, and centrifuged to remove particulate.<br>Extracts (10 uL) were analyzed with HILIC-LC-MS using an Agilent Poroshell 120 HILIC-Z column (2.1 x 100 mm, 1.9 um particle size) at 35 C. Solvent A: 95/5 water/acetonitrile with 0.2% acetic acid and 5 mM ammonium acetate; Solvent B: 95/5 acetonitrile/water with 0.2% acetic acid and 5 m M ammonium acetate.<br>Gradient (0.3 mL/min):99% B for 1 min, decrease to 40% B over 9 min, increase to 99% B over 6 min.
提供机构:
figshare
创建时间:
2022-08-23
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