Synthesis of Sulfonyl Fluorides Using Direct Chloride/Fluoride Exchange in Potassium Fluoride and Water/Acetone
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https://figshare.com/articles/dataset/Synthesis_of_Sulfonyl_Fluorides_Using_Direct_Chloride_Fluoride_Exchange_in_Potassium_Fluoride_and_Water_Acetone/22280848
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资源简介：
A multitude of synthetic routes are available for the
preparation
of sulfonyl fluorides (R–SO2F) whose discovery is
now almost a century old. These syntheses are often limited by the
scope, hazardous materials, and elaborate procedures. The simple and
mild procedure based on direct chloride/fluoride exchange from a sulfonyl
chloride (R–SO2Cl) starting material in a KF and
water/acetone biphasic mixture is investigated. Seventeen examples
in high yield (84–100%) with wide scope are described.
创建时间：
2023-03-15
