3D ED raw data for "Application-led, online analysis of flow synthesised Metal-Organic Frameworks (MOFs)"

3D ED data for the crystal structure in the title publication (https://doi.org/10.1039/d6ta03191a). Data were collected using continuous rotation in selected area mode. The table below summarizes generic data collection parameters for the data collection. The table below summarizes the data collection parameters: General Collection site University of Southampton Crystal structure deposit 2499142 (2024NEDFSO_0012), 2499143 (2024NEDFSO_0013) Instrumental Instrument Rigaku XtaLAB Synergy-ED, electron diffractometer Radiation source LaB6 filament Accelerating voltage [kV] 200 Wavelength [Å] 0.0251 Probe type Parallel beam (SAED) Beam convergence Parallel beam Detector Rigaku HyPix-ED, hybrid pixel array detector Number of pixels in the image 775 × 385 Pixel size [µm] 100 Hardware binning 1 Sample source synthesis Experimental Data type electron diffraction data - 3D ED Data collection method continuous rotation - cRED Collection temperature [K] 293(5) Sample description Chemical composition C18 H14 Cu O14 (2024NEDFSO_0012); C6 H4 Cu O4.5 (2024NEDFSO_0013) Grid holey carbon coated copper grid, 200 mesh (Agar Scientific, UK) Sample preparation suspension in ethanol, sonicate for 4 min, dropcast on grid, evaporate at 50 °C in air Sample holder JEOL TEM holder with high-tilt retainer Software & Files Software for data collection CrysAlisPro 1.171.43.107a Software for data processing CrysAlisPro 1.171.44.123a (2024NEDFSO_0012); CrysAlisPro 1.171.44.126a (2024NEDFSO_0013) Image folders ./frames/xxx.rodhypix./frames/xxx.tiff Image format .rodhypix.tiff Additional files CrysAlisPro files:./expinfo/./expinfo/exp_XXXX_datacoll.ini./plots_dc.plots_dc/exp_XXX_hypix.dat.plots_dc/exp_XXX_Jeol_MicroED.dat.plots_dc/exp_XXX_primarybeam.dat.plots_dc/exp_XXX_primarybeam_0.jpg./CrysalisExpSettings.ini./exp_XXX.par./exp_XXX.run./new.ccdGrain snapshots files:./exp_XXXX_microed_grain_snapshot.rodhypix./exp_XXXX_microed_grain_snapshot.tiff./exp_XXXX_microed_grain_snapshot.jpg