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Improved route to a diphenoxide-based precursor for CVD of parylene AF-4

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http://datadryad.org/dataset/doi%253A10.5061%252Fdryad.tx95x69wc
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资源简介:
In this work, we present an easy synthesis of a alternative precursor for CVD of parylene AF-4 to the widely used standard, Octafluoro[2.2]paracyclophane. The standard precursor suffers from uncertainties in its supply chain and its synthesis is of low yield. A comparison between different reaction parameters and solvents are being discussed by means of thermal, laboratory scale and microwave assisted reactions and qNMR studies. Methods There is GC-MS data available, as well as infrared and various NMR spectra.
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2022-01-19
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