Photocatalytic C(sp3)–C(sp2) radical-polar crossover cross-coupling of styrenyl boronic acids (thesis data)

The attached Data files underpin the publication of my research, described in the following thesis: Photocatalytic C(sp3)–C(sp2) radical-polar crossover cross-coupling of styrenyl boronic acids. The following file types and formats includes: - 1H NMR and 13C NMR of every single molecule synthesised. - 11B and 19F NMR of the structure (if applicable). Every single molecule has a unique number (3.XX) corresponding to a folder containing all the NMR data. NMR data can opened with Mnova or Topspin Instruments 1H, 13C {1H}, 19F {1H} NMR spectra were recorded by either a Bruker AVII 400 (BBFO probe) or AVIII HD 500 or AVIII 500 with BBFO+ and Prodigy BBFO probes, respectively, at 400 101-376 MHz or at 500-126-377 MHz respectively. 11B NMR spectra were recorded on a Bruker AV300 spectrometer at 96 MHz or on a Bruker AVII 400 spectrometer at 128 MHz. All spectra were recorded at room temperature with the deuterated solvents used as a lock for spectra and internal reference (CDCl3: 1H, 7.26 ppm; 13C, 77.2 ppm; acetone-d6: 1H, 2.05 ppm, 13C, 29.8 ppm; d6-DMSO-d6: 1H, 2.50 ppm, 13C, 39.5 ppm; MeCN-d3: 1H, 1.94 ppm, 13C, 1.3 ppm)