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Synthesis of Macrocyclic β-Strand Templates by Ring Closing Metathesis

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NIAID Data Ecosystem2026-03-06 收录
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https://figshare.com/articles/dataset/Synthesis_of_Macrocyclic_Strand_Templates_by_Ring_Closing_Metathesis/2851606
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资源简介:
We report the synthesis of macrocycles 1−6 via ring closing metathesis of dienes 7−12. Addition of chlorodicyclohexylborane to thermal and microwave assisted RCM of dienes 8 and 9 markedly improves the yield. The geometric isomers of macrocycles 1−3 and 5 have been assigned using X-ray crystallography and NMR.
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2009-06-05
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