入厂大米中总砷含量的检验结果评定数据
收藏浙江省数据知识产权登记平台2023-11-22 更新2024-05-08 收录
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砷是一种非金属元素,毒性与重金属相似。,会影响发育,引发心脏疾病、糖尿病,以及损害神经系统和大脑。这种有毒元素可以通过水和土壤被作物吸收,并进入食物链。测定入厂大米中总砷含量是否达到国家标准,提前做好大米的入厂筛选工作,为消费者的安全做好监测工作。以国家标准GB2762-2012为检验依据,采用原子荧光光度法测定大米中总砷的
含量,所用试剂有砷标准溶液(国家标准物质中心)1000ug/mL,记录试样被测液的浓度C1(μg/L),试剂空白液的浓度C0(μg/L)和消化液总体积V(ml),称取大米试样质量m1.5g于锥形瓶中,加入硝酸和硫酸,摇匀过夜后在电热板上加热消解,消解不完全,就加入高氯酸,持续蒸发,冷却后加水再蒸至冒硫酸白烟,冷却,用水转移至容量瓶中加入硫脲定容,测得大米中总砷的含量,计算公式如下:总砷含量X(mg/kg)=[(C1-C0)/m]*(V/标准溶液1000);结果与标准中的规定一致,判定公式:F(x)=IF(入厂大米总砷含量测定值<0.2mg/kg,"合格","不合格")。
Arsenic is a non-metallic element with toxicity similar to that of heavy metals. It can impair development, induce cardiovascular diseases and diabetes, and damage the nervous system and brain. This toxic element can be absorbed by crops through water and soil, and enter the food chain. To verify whether the total arsenic content in incoming rice complies with national standards, pre-screening of incoming rice shall be carried out to monitor consumer safety. Based on the national standard GB2762-2012, atomic fluorescence spectrometry was employed to determine the total arsenic content in rice. The reagents used include arsenic standard solution (from the National Standard Material Center) at a concentration of 1000 μg/mL. Record the concentration of the sample test solution C1 (μg/L), the concentration of the reagent blank solution C0 (μg/L), and the total volume of the digested solution V (mL). Weigh 1.5 g of rice sample (denoted as m, unit: g) into a conical flask, add nitric acid and sulfuric acid, shake thoroughly and allow to stand overnight, then heat for digestion on an electric hot plate. If the digestion is incomplete, add perchloric acid and continue evaporation. After cooling, add water and evaporate until sulfuric acid fumes evolve, then cool again. Transfer the solution quantitatively to a volumetric flask using water, add thiourea and adjust to the final volume. The total arsenic content X (mg/kg) is calculated as follows: X (mg/kg) = [(C1 - C0) / m] × (V / 1000). Where the measured result conforms to the standard provisions, the judgment formula is: F(x) = IF(measured total arsenic content of incoming rice < 0.2 mg/kg, "qualified", "unqualified");
提供机构:
台州市军融农业发展股份有限公司
创建时间:
2023-11-08
搜集汇总
数据集介绍

特点
该数据集包含298条入厂大米中总砷含量的检验结果评定数据,用于测定大米中总砷含量是否达到国家标准GB2762-2012。数据采用原子荧光光度法测定,并根据标准限量指标评定合格与否,应用场景为保障消费者安全。
以上内容由遇见数据集搜集并总结生成



