MoS2 Lithiation Mechanism - Electrochemistry & Ex situ Material Characterisation

Digital ImagesPristine Electrode Laminates.Ex Situ Electrode (in Glovebox) - after Lithiation versus a lithium metal counter electrode.Electrochemical Data (.mpt)Ex situ cells discharged to D1 0.80V, D1 0.40V, D1 0.01V, and C1 3.00V with MoS2 electrodes of 12 um, 36 um, and 87 um thickness.Ex situ cells (36 um) MoS2 (3.00 -0.01 V) cycled for 11 and 51 cycles.SEMPristine MoS2 electrodes of 12 um, 36 um, and 87 um thicknessEx situ cycled MoS2 electrodes of 36 um (D1 0.80V, D1 0.01V, and C1 3.00V)XRD (Cu Source)Pristine MoS2 electrode 36 umEx situ cycled MoS2 electrodes of 36 um (D1 0.80V, D1 0.01V, and C1 3.00V)Raman Spectroscopy (air-free holder, 785 nm)Pristine MoS2 electrode 36 umEx situ cycled MoS2 electrodes of 36 um (D1 0.80V, D1 0.01V, and C1 3.00V)XPS (air-free)Pristine MoS2 electrode 36 umEx situ cycled MoS2 electrodes of 36 um (D1 0.80V, D1 0.01V, and C1 3.00V)