Plasma-based synthesis of Re, Ir, Pd, and Rh nanocluster catalysts and their potential in the catalytic reduction processes

The collection contains a set of data related to the synthesis of d-block element nanocluster catalysts selected from the group Re, Ir, Pd, and Rh.For the synthesis, a new, 3D-printed plasma reactor operating with direct current atmospheric glow discharge was used. The series of catalysts was used for the catalytic reduction of 4-nitrophenol, resulting in the synthesis of 4-aminophenol.The research was carried out within the Opus 25 project (UMO-2023/49/B/ST8/01029) granted by the National Science Centre (Poland). The aim of the project is to develop a new generation of catalytic technology for the production of aromatic amines.The set of data contains:DLS (dynamic light scattering) data associated with hydrodynamic diameters, polydispersity index, and particle diameter.ELS (electrophoretic light scattering) data associated with zeta potential and conductivity.Transmission electron microscopy images of the synthesized catalysts.Elemental surface composition obtained during TEM/EDX analysis.UV-Vis spectra recorded during catalytic reactions carried out in a batch mode.