Assignment of the NMR spectroscopic signals observed for 5′PRib1′2NAcAmEtPn.<sup>a</sup>
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aThe preparation also contained 2NAcAmEtPn and small amounts of one or more contaminants. 13C and 1H NMR spectra were assigned to correlations observed in the COSY, HSQC and HMBC NMR spectra. 1H/13C and 1H/31P HMBC NMR correlations are shown. b2H of 5′PRib1′2NAcAmEtPn and 2NAcAmEtPn, each, as well as 3H from contamination. cH2′ and H3′ as well as H from contamination. dData for 2NAcAmEtPn.
创建时间:
2012-10-03



