Type II PLC Paper Draft Data

To map the following data, use the key and mapping routes below:

Key;

   Concentration in unsealed environment:

      30 wt%:  “1”

      25 wt%:  “4”

      20 wt%:  “7”

      15 wt%:  “10”

      10 wt%:  “13”

      5 wt%:    “19”

      2.5 wt%: “22”

   Concentration in partially sealed environment:

      30 wt%:  “2”

      25 wt%:  “5”

      20 wt%:  “8”

      15 wt%:  “11”

      10 wt%:  “14”

      5 wt%:    “20”

      2.5 wt%: “23”

   Concentration in fully sealed environment:

      30 wt%:  “3”

      25 wt%:  “6”

      20 wt%:  “9”

      15 wt%:  “12”

      10 wt%:  “15”

      5 wt%:    “21”

      2.5 wt%: “24”

   Solvent at 292-294 K storage temperature:

      PCP: “A”

      TBA: “C”

      MS:  “E”

      DCT: “G”

      HAP:”I”

   Solvent at 277 K storage temperature:

      PCP: “B”

      TBA: “D”

      MS:  “F”

      DCT: “H”

      HAP:”IJ”

Initial Screen:

   To map the Initial Screen data:

      An example:

         select the solvent at the chosen storage temperature: “A” (ignore all references to “R#”)

         select the concentration at the chosen evaporation rate: “9A”

      The coordinates of the LTS420 stage are given in the format “x-y”, where each coordinate is split into two, for example “01” can be either “01.0” or “01.5” to represent the first and second half of “01” between “01” and “02”. Each half is then differentiated by 50 positions ranging from “00” to “49”, meaning that within “01.0” there are 50 different coordinates from “01.0.00” to “01.0.49”.

   To read the nomenclature of the files:

      An example:

         concentration at chosen evaporation rate: “9”

         solvent at chosen storage temperature: “A”

         day micrograph was taken relative to the day the sample was prepared: “D3”

         temperature at time micrograph was taken: “T21”

         coordinates on LTS420 stage when micrograph was taken: “10.0.18-10.5.14”

         magnification lens used to capture micrograph: “10x”

         if applicable, optical image: “O”

         overall name: “9A-D3-T21-10.0.18-10.5.14-10x”

Water Screen:

   To map the Water Screen data:

      An example:

         select the solvent at the chosen storage temperature: “C”

         select the water content at the given concentration and evaporation rate: “0.8H2O”

      The coordinates of the LTS420 stage are given in the format “x-y”, where each coordinate is split into two, for example “01” can be either “01.0” or “01.5” to represent the first and second half of “01” between “01” and “02”. Each half is then differentiated by 50 positions ranging from “00” to “49”, meaning that within “01.0” there are 50 different coordinates from “01.0.00” to “01.0.49”.

   To read the nomenclature of the files:

      An example:

         concentration at given evaporation rate: “8”

         solvent at given storage temperature: “C”

         water content: “0.8H2O”

         day micrograph was taken relative to the day the sample was prepared: “D8”

         temperature at time micrograph was taken: “T21”

         coordinates on LTS420 stage when micrograph was taken: “07.0.05-11.0.10”

         magnification lens used to capture micrograph: “5x”

         if applicable, optical image: “O”

         overall name: “8C-0.8H2O-D8-T21-07.0.05-11.0.10-5x”

Porous Organic Cage (POC) Composition Screen:

   To map the POC Composition Screen data:

      An example:

         select the solvent at the chosen storage temperature: “H”

         select the POC composition at the given concentration and evaporation rate: “2”

      The POC compositions are from 1-5 where:

         CC33.25:132.75-R:  “1”

         CC33.5:132.5-R:     “2”

         CC33.75:132.25-R: “3”

         CC34:132-R:          “4”

         CC35:131-R:          “5”

      The coordinates of the LTS420 stage are given in the format “x-y”, where each coordinate is split into two, for example “01” can be either “01.0” or “01.5” to represent the first and second half of “01” between “01” and “02”. Each half is then differentiated by 50 positions ranging from “00” to “49”, meaning that within “01.0” there are 50 different coordinates from “01.0.00” to “01.0.49”.

   To read the nomenclature of the files:

      An example:

         concentration at given evaporation rate: “7”

         solvent at given storage temperature: “H”

         POC composition: “2”

         day micrograph was taken relative to the day the sample was prepared: “D10”

         temperature at time micrograph was taken: “T21”

         coordinates on LTS420 stage when micrograph was taken: “14.5.46-14.5.00”

         magnification lens used to capture micrograph: “5x”

         if applicable, optical image: “O”

         overall name: “7H2-D10-T21-14.5.46-14.5.00-5x”

Reproducibility Screen:

   To map the Reproducibility Screen data:

      An example:

         select the chosen concentration and solvent at the given storage temperature: “1G”

         select the POC batch: “047-1”

      The coordinates of the LTS420 stage are given in the format “x-y”, where each coordinate is split into two, for example “01” can be either “01.0” or “01.5” to represent the first and second half of “01” between “01” and “02”. Each half is then differentiated by 50 positions ranging from “00” to “49”, meaning that within “01.0” there are 50 different coordinates from “01.0.00” to “01.0.49”.

   To read the nomenclature of the files:

      An example:

         concentration at given evaporation rate: “1”

         solvent at given storage temperature: “G”

         POC batch: “047-1”

         day micrograph was taken relative to the day the sample was prepared: “D6”

         temperature at time micrograph was taken: “T21”

         coordinates on LTS420 stage when micrograph was taken: “01.5.27-08.5.29”

         magnification lens used to capture micrograph: “5x”

         if applicable, optical image: “O”

         overall name: “1G-047-1-D6-T21-01.5.27-08.5.29-5x”