Table 1 1 H in Metabolite pattern in root nodules of the actinorhizal plant Casuarina equisetifolia

Table 1 1 H (500 MHz) and 13 C NMR (125 MHz) data of compound 1 in CDCl. 3
No.δ Cδ HNo.δ Cδ H137.3, t0.97 a, 1.61 a2028.8, s223.4, t1.57 a2133.1, t1.25 a, 1.33 a381.1, d4.46 (dd, J = 10.7, 5.42235.1, t1.02 a, 1.38 aHz)437.9, s2327.9, q0.78 (s) a555.6, d0.86 a2416.6, q0.84 (s) a618.7, t1.46 a, 1.57 a2515.5, q0.95 (s)741.2, t1.35 a, 2.02 a2625.9, q1.08 (s)839.0, s2721.3, q0.90 (s)949.2, d1.42 a2829.8, q0.82 (s)1037.7, s2933.3, q0.94 (s)1117.5, t1.48 a, 1.63 a3029.9, q0.91 (s)1233.7, t1.61 a1′172.8, s1337.5, s2′36.5, t2.58 (t, J = 7.8Hz)14158.0, s3′30.2, t2.88 (t, J = 7.8Hz)15116.9,5.53 (dd, J = 8.2, 3.24′132.8, sdHz)1637.7, t1.61 a, 1.92 a5′,9′129.4,7.07 (d, J = 8.4dHz)1735.8, s6′,8′115.3,6.74 (d, J = 8.4dHz)1848.7, d0.95 a7′153.9, s1936.6, t0.96 a, 1.31 a
a Assignments were based on HSQC experiment.