Synthesis and X-ray Crystal Structure of [(C<sub>5</sub>Ph<sub>5</sub>)CrCl(μ-Cl)<sub>2</sub>Tl]<sub>2</sub>: An Example of the Rare M−X−Tl<sup>I</sup> Linkage (X = Halide)
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Reaction of solid TlCl with [(C5Ph5)CrCl(μ-Cl)]2 in CH2Cl2 solvent yields the dimeric complex [(C5Ph5)CrCl(μ-Cl)2Tl]2 in 80% isolated yield. The C5H5 and C5Me5 analogues do not react with TlCl, suggesting a steric basis for the reaction of the C5Ph5 material.
创建时间：
2007-09-10
