Nickel-Catalyzed Oxidative Coupling of Unactivated C(sp<sup>3</sup>)–H Bonds in Aliphatic Amides with Terminal Alkynes
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In this work, we demonstrated Ni-catalyzed oxidative coupling of unactivated C(sp3)–H bonds with terminal alkynes for construction of C(sp3)–C(sp) bonds to synthesize alkyl-substituted internal alkynes. Different amides exhibited good compatibility. Preliminary mechanistic studies were conducted to account for this alkynylation.
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2016-10-10
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