Quantitative three-dimensional local order analysis of nanomaterials through electron diffraction
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Diffraction data for Yttrium Stabilized Zirconia Zr<sub>0.82</sub>Y<sub>0.18</sub>O<sub>1.91</sub> <strong>Electron diffraction data:</strong> FEI Tecnai G2 microscope 200 keV electrons Cheetah detector (ASI, 512 x 512 pixel) Condenser Aperature 10 micrometer, spot size 9 Exposure 1.512 s / frame, rotation 0.4 deg/frame raw data was processed with PETS2 (http://pets.fzu.cz/) <strong>X-ray diffraction data:</strong> Rigaku Syneergy S diffractometer Eiger 1M Detector, energy discriminating threshold 17.4 keV Mo K-alpha radiation 120 s exposure time, 0.5 deg/frame Raw data can be processed with CrysAlisPro (https://www.rigaku.com/products/crystallography/crysalis) <strong>Neutron diffraction data:</strong> D19 ILL, Grenoble 0.95 A wavelength 80 s exposure time, 0.1 deg/frame Raw data can be accessed at doi:10.5291/ILL-DATA.5-13-277 and processed with the Instrument software Int3D (https://www.ill.eu/users/instruments/instruments-list/d19/software) <strong>Reciprocal space reconstructions and 3D-DeltaPDF maps</strong> Provided in .h5 format and can be vizualized e.g. with DISCUS (https://github.com/tproffen/DiffuseCode/releases) or DensityViewer (https://github.com/aglie/DensityViewer/releases/)



