The First Mixed-Valent Antimony(III/V) Oxo Clusters (2,6-Mes2C6H3Sb)2(ClSb)4O8 and (2,6-Mes2C6H3Sb)4(ClSb)4(HOSb)2O14†
收藏Figshare2007-07-16 更新2026-04-28 收录
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https://figshare.com/articles/dataset/The_First_Mixed-Valent_Antimony_III_V_Oxo_Clusters_2_6-Mes_sub_2_sub_C_sub_6_sub_H_sub_3_sub_Sb_sub_2_sub_ClSb_sub_4_sub_O_sub_8_sub_and_2_6-Mes_sub_2_sub_C_sub_6_sub_H_sub_3_sub_Sb_sub_4_sub_ClSb_sub_4_sub_HOSb_sub_2_sub_O_sub_14_sub_sup_s/12077889
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The kinetically controlled base hydrolysis of the sterically encumbered arylantimony dichloride 2,6-Mes2C6H3SbCl2 (1) under aerobic conditions afforded [2,6-Mes2C6H3(Cl)SbIII]2O (2) and the mixed-valent clusters (2,6-Mes2C6H3SbV)2(ClSbIII)4O8 (3) and (2,6-Mes2C6H3SbV)4(ClSbIII)4(HOSbIII)2O14 (4), whose molecular structures are dominated by hypervalent and secondary bonding.
创建时间：
2007-07-16
