Synthesis of the 1,2,4-Thiadiazole Alkaloid Polyaurine B
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https://figshare.com/articles/dataset/Synthesis_of_the_1_2_4-Thiadiazole_Alkaloid_Polyaurine_B/12136806
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A short synthesis of the natural product polyaurine B is described. The 1,2,4-thiadiazole heterocycle was assembled using a Cu(II)-mediated heterocyclization reaction that forges the N–S bond. The final acylation step to install the methylcarbamate must be conducted under anhydrous, nonbasic conditions to prevent thiadiazole ring opening initiated by attack of hydroxide at C-5.
创建时间：
2020-04-16
