Absolute Configuration of 2-(Tributylstannyl)pyrrolidine by Anomalous Dispersion X-ray Analysis
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https://figshare.com/articles/dataset/Absolute_Configuration_of_2_Tributylstannyl_pyrrolidine_by_Anomalous_Dispersion_X_ray_Analysis/3305614
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资源简介：
Enantiopure 2-(tributylstannyl)pyrrolidine hydroiodide may
be prepared in excellent yield by TMSI treatment of the
corresponding N-Boc compound, which is in turn prepared
by asymmetric deprotonation (s-BuLi·sparteine) and stannylation, as described in the literature. Crystals of the
hydroiodide salt suitable for X-ray analysis were obtained,
and although there is some disorder about the butyl groups,
analysis using anomalous dispersion establishes the absolute
configuration as S.
创建时间：
2016-05-06
