Tetrasilane-Bridged Bicyclo[4.1.0]heptasil-1(6)-ene
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https://figshare.com/articles/dataset/Tetrasilane_Bridged_Bicyclo_4_1_0_heptasil_1_6_ene/2254360
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资源简介：
Tetrasilane-bridged bicyclo[4.1.0]heptasil-1(6)-ene 1 was synthesized by the reduction of 1,1,2,2-tetrachlorocyclohexasilane 2 in 12% yield as red-orange crystals. The structure and properties of 1 were studied by spectroscopy, X-ray crystallography, and theoretical calculations. The linkage of the cyclotrisilene moiety with two tetrasilane chains with tert-butyl groups remarkably affects its structure and 29Si NMR spectrum.
创建时间：
2016-02-16
