遇见数据集

国际标样BHVO-2、TDB-1、GPt-4、UMT-1、WPR-1的Re-Os同位素和PGE含量数据

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国家青藏高原科学数据中心2025-12-11 更新2025-12-20 收录
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本数据包含国际标样BHVO-2、TDB-1、GPt-4、UMT-1、WPR-1的Re-Os同位素和PGE含量数据,数据来源为2020YFA0714802,在国家地质实验测试中心完成测试。将国际标准物质样品经Carius管溶样-同位素稀释法及化学前处理后各元素分别进行测量,Re采用多接收等离子体质谱测量、Os采用热表面电离质谱测量、PGE采用Agilent 8900-ICP-MS/MS测量。采用Re同位素比值标准溶液,使用SSB法对多接收等离子体质谱获得的Re同位素比值进行分馏校正。采用国家标准物质JCBY对Re-Os同位素数据进行全流程监控。采用实验室内部监控溶液std系列元素标准溶液及PGE混合标准溶液对ICP-MS/MS获得的PGE数据进行干扰元素及同质异位素进行监控及数据校正。所有数据误差以2σ给出。其应用前景广泛且具有重要学术与实际价值:一是为全球地质分析实验室提供校准基准,可用于验证 Re-Os 同位素定年及 PGE 含量测试方法的准确性、重复性,支撑实验室质量控制体系建设;二是助力跨区域、跨机构数据对比与整合,国际标样的统一数据参考能打破不同研究团队的技术壁垒,推动全球岩浆演化、矿产资源成因等领域的协同研究;三是促进分析方法标准化与技术推广,为我国地质实验测试行业制定 Re-Os/PGE 分析标准方法提供核心数据依据,助力国内技术与国际接轨。

This dataset contains Re-Os isotope and Platinum Group Elements (PGE) content data for international standard reference materials BHVO-2, TDB-1, GPt-4, UMT-1, and WPR-1. The data was sourced from project 2020YFA0714802 and tested at the National Research Center for Geoanalysis. International standard reference material samples were dissolved via Carius tube isotope dilution method, followed by chemical pretreatment, before individual elements were measured separately. Re was analyzed using multi-collector inductively coupled plasma mass spectrometry (MC-ICP-MS), Os using thermal ionization mass spectrometry (TIMS), and PGE using Agilent 8900 ICP-MS/MS. Re isotope ratio standard solutions were employed, and the Sample Standard Bracketing (SSB) method was applied to correct for mass fractionation of Re isotope ratios obtained by MC-ICP-MS. National standard reference material JCBY was used to conduct full-workflow monitoring of Re-Os isotope data. Internal laboratory monitoring solutions, including the std-series elemental standard solutions and PGE mixed standard solutions, were utilized to monitor and correct for interfering elements and isobars in PGE data acquired by ICP-MS/MS. All data errors are reported as 2σ. This dataset has broad application prospects and considerable academic and practical value: Firstly, it provides calibration benchmarks for global geological analysis laboratories, which can be used to verify the accuracy and repeatability of Re-Os isotope dating and PGE content testing methods, supporting the establishment of laboratory quality control systems. Secondly, it facilitates cross-regional and cross-institutional data comparison and integration. The unified data reference of international standard reference materials can break technical barriers among different research teams, promoting collaborative research in fields such as global magmatic evolution and mineral resource genesis. Thirdly, it promotes the standardization of analytical methods and technology popularization, providing core data support for formulating Re-Os/PGE analytical standard methods in China's geological experimental testing industry, and helping domestic technologies align with international standards.

创建时间:
2025-12-01
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