single crystal X-ray diffraction (single-crystal X-ray diffraction) ()

dataset for single crystal X-ray diffraction (single-crystal X-ray diffraction) Single crystals suitable for X-Ray analysis were obtained by slow evaporation of methanol from a solution with the metal complex under ambient pressure.Crystal Data for C29H30AgF3N10O3S (M =763.56 g/mol): monoclinic, space group P21/n (no. 14), a = 14.1441(4) Å, b = 15.5702(4) Å, c = 15.1099(4) Å, β = 111.231(2)°, V = 3101.75(15) Å3, Z = 4, T = 150 K, μ(GaKα) = 4.281 mm-1, Dcalc = 1.635 g/cm3, 32166 reflections measured (7.364° ≤ 2Θ ≤ 124.964°), 7415 unique (Rint = 0.0200, Rsigma = 0.0133) which were used in all calculations. The final R1 was 0.0285 (I > 2σ(I)) and wR2 was 0.0745 (all data).