Thermal behavior of (NH4)V4O10xH2O

The DataSet contains the results of the thermal behavior of the (NH4)V4O10xH2O obtained by the hydrothermal method using different precursors: microstructured (commercially available) or nanostructured. The information about samples synthesis is described in the Materials. Thermogravimetric analysis (TG) under synthetic air atmosphere from 40°C to 905°C (with a heating rate of 5 °C/min) using Netzsch STA 449 F1. The thermal behavior was also studied with mass spectrum (MS). The gases that come out from the samples during heating were monitored by the quadruple mass spectrometer Netzsch QMS 403C Aeolos. The mass spectra were measured in the m/z range from 2 to 60.