Synthesis and Direct C2 Functionalization of Imidazolium and 1,2,4‑Triazolium N‑Imides
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https://figshare.com/articles/dataset/Synthesis_and_Direct_C2_Functionalization_of_Imidazolium_and_1_2_4_Triazolium_i_N_i_Imides/2237632
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Pd-catalyzed direct C2 arylation and Cu-catalyzed direct one-pot alkynylation/intramolecular cyclization of azolium N-imides are reported. Various acetylenes, aryl iodides, and 1-alkyl substituents were examined. The mild protocol allows direct C2 arylation of azolium N-imides without the use of specialized reagents together with novel one-pot regioselective preparations of imidazole-pyrazolo and pyrazolo-1,2,4-triazole ring systems. The electronic properties of selected examples were examined by fluorescence spectroscopy.
创建时间：
2016-02-16
