Building a cost-effective mechanochemical Raman system: improved spectral and time resolution for in situ reaction and rheology monitoring - dataset

This dataset comprises Raman spectroscopy data collected using our in-house Raman spectrometer for in situ reaction and rheology monitoring of a benchmark mechanochemical reaction. It also includes Raman spectra obtained with two commercial Raman spectrometers for comparison, as well as PXRD data to analyze the structure of the reaction products. Additionally, the dataset contains data required for the characterization and calibration of the in-house Raman spectrometer. The data are organized to correspond directly with the images presented in the article (Main text and Supporting Information). The collection includes experimental raw data (X-Y sets, image files) and the Python scripts used for data processing.