Single-crystal X-ray diffraction dataset for 2,6-diaminopurine dithymine dihydrate
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https://repod.icm.edu.pl/citation?persistentId=doi:10.18150/repod.6829666
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The crystals of the title compound were obtained by heating a solution of 2,6-diaminopurine and thymine in distilled water and slow evaporation of the solvent. Single needle crystal was selected and mounted with paratone-N oil to the MiTiGen micro-mount. The crystal was kept at 100.00(12) K during diffraction data collection on the Rigaku Oxford Diffraction (former Agilent Technologies) SuperNova four-circle diffractometer with CuKα radiation and Atlas detector. The temperature was controlled with an Oxford Cryosystems low-temperature nitrogen gas-flow device (Cryostream Plus). The crystal was positioned at 74 mm from the detector. A total of 1209 frames were collected in 23 runs using ω scan; rotation width of 1.0° and exposure time in the range of 5 - 30 seconds.
提供机构：
RepOD
创建时间：
2017-09-15
