One-Pot Synthesis of Aminoenone via Direct Reaction of the Chloroalkyl Enone with NaN<sub>3</sub>: Rapid Access to Polycyclic Alkaloids
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A new one-pot procedure for the preparation of aminoenone from chloroalkyl enone and sodium azide was demonstrated. The structure of the presumed triazoline intermediate in this process was confirmed by X-ray analysis for the first time. As the application of this methodology, the synthesis of polycyclic alkaloid hexahydroapoerysopine (1a) was achieved through an efficient synthetic route.
创建时间：
2010-08-06
