Reduction of CO<sub>2</sub> into Methylene Coupled with the Formation of C–S Bonds under NaBH<sub>4</sub>/I<sub>2</sub> System
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A selective four-electron reduction of CO2 with thiophenol using NaBH4 as a reductant is described to access dithioacetals. This reaction provides a novel synthetic method for the highly selective conversion of CO2 into methylene, and a new access to molecular structures via formation of C–S bonds using CO2 as the C1 source.
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2018-10-11
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