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Freeze-drying protocols as used in this study (PD = primary drying, and SD = secondary drying).

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https://figshare.com/articles/dataset/Freeze-drying_protocols_as_used_in_this_study_PD_primary_drying_and_SD_secondary_drying_/3958494
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The pressure rise test (PRT) in cycle I was used to confirm the end of primary drying. In cycle II the PRT was used during primary drying and after not meeting the criterion (maximum rise in pressure <0.03 mbar/min) the primary drying stage was prolonged by an additional 2 hours.
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2016-09-29
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