Freeze-drying protocols as used in this study (PD = primary drying, and SD = secondary drying).
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The pressure rise test (PRT) in cycle I was used to confirm the end of primary drying. In cycle II the PRT was used during primary drying and after not meeting the criterion (maximum rise in pressure <0.03 mbar/min) the primary drying stage was prolonged by an additional 2 hours.
创建时间：
2016-09-29
