Publication raw data: “Zirconia functionalized monolithic cores with improved hierarchical porosity for continuous-flow microreactors in cascade reactions”

File:ASAPFile format: *csvFigure 1, 2, Table 1Data from nitrogen adsorption/desorption measurements.Isotherms and Pore Size Distribution (PSD)ASAP2020 Micromeritics; ASAP2020 softwereSamples degassed at 200 ◦C under vacuum for 24 h. Nitrogen adsorption at −196◦C. The specific surface area calculated using Braunauer, Emmet and Teller (BET) equation.File:TGFile format: *csvData from thermogravimetric measurements of samples modified with amines: TG curves (%mass loss).Star 850, Mettler Toledo. Temperature range of 25-800 °C, heating ramp of 10 deg/min, air flow rate: 60 ml/minFile:Flow resistanceFile format: *csvFigure 3Data from flow resistance measurements.Pressure controller UNIK 5000, Ex-Calibra, syringe pump.File:RTDFile format: *csvFigure 4, Table 2Data from residence time distribution evaluation. Syrgine Pump, Temperature 25°C, 4 cm long microreactors with NH2-SIO2 or ZrO2-SiO2 monolithic cores. Sampling:0.5-1 min.File:Catalytic ResultsFile format:*csvFigure 5Signals from GC chromatographyAgilent 7890A, flame ionization detector FID; capillary column HP5; Inlet temperature: 250◦C ; sample volume: 1um, split ratio: 5:1; oven temp: 40◦C-200o◦C He flow 6.5 ml/min; detector: temperature 300◦C; H2 flow:30 ml/min, Air flow:400ml/min