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Synthesis of Functionalized Acenaphthenes and a New Class of Homooxacalixarenes

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https://figshare.com/articles/dataset/Synthesis_of_Functionalized_Acenaphthenes_and_a_New_Class_of_Homooxacalixarenes/2507644
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The 5,6-dialkoxyethers of acenaphthene have been synthesized for the first time via modified Ullmann reaction conditions. Further modifications of the 5,6-dimethoxyacenaphthene allowed the synthesis of the first acenaphthene analogue of the octahomotetraoxacalixarenes. The X-ray structure of this new macrocycle and its complexation study with C60 are reported.
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2012-07-06
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