Reductive Silylation of the Uranyl Ion with Ph3SiOTf
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https://figshare.com/articles/dataset/Reductive_Silylation_of_the_Uranyl_Ion_with_Ph_sub_3_sub_SiOTf/2230702
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The reaction of 2 equiv of Ph3SiOTf with UO2(dbm)2(THF) (dbm = OC(Ph)CHC(Ph)O) and UO2(Aracnac)2 (Aracnac = ArNC(Ph)CHC(Ph)O; Ar = 3,5-tBu2C6H3) results in the formation of U(OSiPh3)2(dbm)2(OTf) (1) and [U(OSiPh3)2(Aracnac)2][OTf] (2), respectively, in good yield.
创建时间：
2016-02-16
