3D ED raw data for "Structure–property relationships in disodium anthracene dicarboxylate for sodium-ion storage via 3D electron diffraction"

3D ED data for the crystal structure in the title publication (https://doi.org/10.1039/D5CC03175C). Data were collected using continuous rotation in selected area mode. The table below summarizes generic data collection parameters for the data collection. Collection site University of Southampton, NCS/NEDF Sample label(s) 2024NCS0534 Crystal structure deposit CSD 2415532 Instrumental Instrument Rigaku XtaLAB Synergy-ED, electron diffractometer Radiation source LaB6 Accelerating voltage [kV] 200 Wavelength [Å] 0.0251 Probe type Parallel beam (SAED) Beam convergence Parallel beam Detector Rigaku HyPix-ED, hybrid pixel array detector Number of pixels in the image 775 x 385 Pixel size [µm] 100 Hardware binning 1 Sample description Name Na2-ADC Chemical composition C16 H8 Na2 O4 Sample source Synthesis Grid lacey carbon coated copper grid, 200 mesh (Agar Scientific) Sample preparation Sample ground between glass slides, grid dabbed, cryo transfer @ 175 K Sample holder GATAN Elsa cryo-transfer holder 698 Experimental Data type Electron diffraction data - 3D ED Data collection method Continuous rotation - cRED Collection temperature [K] 175 Software Software used for the data collection CrysAlisPro 1.171.44.65a Software used for processing CrysAlisPro 1.171.44.65a Files and data formats Image folders ./frames/xxx.rodhypix./frames/TIFF/xxx.tiff Image format .rodhypix.tiff (converted with CrysAlisPro) Additional files CrysAlisPro files: ./expinfo/./expinfo/exp_XXXX_datacoll.ini ./plots_dc.plots_dc/exp_XXX_hypix.dat.plots_dc/exp_XXX_Jeol_MicroED.dat.plots_dc/exp_XXX_primarybeam.dat.plots_dc/exp_XXX_primarybeam_0.jpg ./CrysalisExpSettings.ini./exp_XXX.par./exp_XXX.run./new.ccd Grain snapshots files: ./exp_XXXX_microed_grain_snapshot.rodhypix./exp_XXXX_microed_grain_snapshot.tiff