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https://zenodo.org/record/7590188

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The following submission contains the data collection frames for the sample Natrolite under the NanED round-robin project. Precession Electron Diffraction (PED) as well as Continuous Rotation Electron Diffraction were carried out on two different single crystal. The datasets were processed with PETS2 and XDS software and refined both kinematically and dynamically using Jana. The table below summarizes the data collection parameters for the data sets. Continuous Rotation: General Information Project NanED (www.naned.eu) ESR Project ESR1 & ESR2 Instrumental Instrument Zeiss Libra 120 Radiation source LaB6 Accelerating voltage 120 kV Wavelength 0.0335 Å Probe Type Nanodiffraction Beam Diameter 600 nm Beam Convergence Parallel beam Detector Timepix Single Electron Detector Number of pixels in the image 512 x 512 Physical pixel size 55 µm * 55 µm Effective camera length 144 mm Calibration constant 0.006027 Å-1/pixel Sample description Name Natrolite Chemical composition Na2Al2Si3O10·2H2O Sample source Natural sample from Marianska Skala, Usti nad Labem, Czechia Sample preparation Crushed with a mortar and diluted using isopropanol before depositing a drop on a Cu grid. Experimental Data type 3D Electron Diffraction (3D-ED) Data collection method Continuous Rotation Electron Diffraction (CRED) Rotation Speed 2.00 º/s Temperature 293 K Number of crystals contributing to the dataset 1 Number of experimental frames 293 Tilt range, tilt step -60º to +55, 0.4º Exposure time per frame 200 ms Software Software used for data collection WinTEM (Zeiss), Digistar (NanoMEGAS) and Sophy (Software for Physics) Software used for processing XDS Software used for solution Shelxt Software used for refinement Jana Authorship and bibliography Author(s) of the data Moussa Diame FAYE (ESR1) & Vincentia Emerson Agbemeh (ESR2) Related data Publication(s) Precession: General Information Project NanED (www.naned.eu) ESR Project ESR1 & ESR2 Instrumental Instrument Zeiss Libra 120 Radiation source LaB6 Accelerating voltage 120 kV Wavelength 0.0335 Å Probe Type Nanodiffraction Beam Diameter 150 nm Beam Convergence Parallel beam Detector Timepix Single Electron Detector Number of pixels in the image 512 x 512 Physical pixel size 55 µm * 55 µm Effective camera length 144 mm Calibration constant 0.006027 Å-1/pixel Sample description Name Natrolite Chemical composition Na2Al2Si3O10·2H2O Sample source Natural sample from Marianska Skala, Usti nad Labem, Czechia Sample preparation Crushed with a mortar and diluted using isopropanol before depositing a drop on a Cu grid. Experimental Data type 3D Electron Diffraction (3D-ED) Data collection method Precession Precession Semiangle 1º Temperature 293 K Number of crystals contributing to the dataset 1 Number of experimental frames 116 Tilt range, tilt step -59º to +55, 1º Exposure time per frame 1000 ms Software Software used for data collection WinTEM (Zeiss), Digistar (NanoMEGAS) and Sophy (Software for Physics) Software used for processing PETS2 Software used for solution SIR2019 Software used for refinement Jana Authorship and bibliography Author(s) of the data Moussa Diame FAYE (ESR1) & Vincentia Emerson Agbemeh (ESR2) Related data Publication(s)

应用场景：

Natrolite - Sample 2 NanED, Data ESR1 & ESR2