X-ray diffraction (XRD) analysis was carried out with a PanAnalytical X’Pert PRO (CuKα radiation), wavelength of 1.54 Å, with operation settings 45 kV and 40 mA.XRD bulk analysis was performed on drie
Method A: wet-bulk volume measured with special volume sampler; method B: wet-bulk volume measured by gas pycnometry; method C: dry volume measured by gas pycnometry
Method A: wet-bulk volume measured with special volume sampler; method B: wet-bulk volume measured by gas pycnometry; method C: dry volume measured by gas pycnometry
