Synthesis of Benzidine Derivatives via FeCl3·6H2O‑Promoted Oxidative Coupling of Anilines
收藏Figshare2016-02-19 更新2026-04-29 收录
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https://figshare.com/articles/dataset/Synthesis_of_Benzidine_Derivatives_via_FeCl_sub_3_sub_6H_sub_2_sub_O_Promoted_Oxidative_Coupling_of_Anilines/2407558
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Under open-flask conditions in the presence of commercially available FeCl3·6H2O, N,N-disubstituted anilines can be converted into diversely functionalized benzidines with yields of up to 99%. Oxidative coupling was extended to N-monosubstituted anilines, and the method was applied to the efficient preparation of 6,6′-biquinoline. Mechanistic investigations have also been performed to explain the observed reactivities.
创建时间：
2016-02-19
